12 results
Search Results
Now showing 1 - 10 of 12
Article Citation - WoS: 13Citation - Scopus: 13Effect of Aging Treatment on the Microstructure, Cracking Type and Crystallographic Texture of In939 Fabricated by Powder Bed Fusion-Laser Beam(Elsevier, 2024) Ozer, Seren; Dogu, Merve Nur; Ozdemirel, Ceren; Bilgin, Guney Mert; Gunes, Mert; Davut, Kemal; Brabazon, DermotThis study aimed to provide a comprehensive understanding of how aging treatments (namely, HT1 and HT2) affect the microstructure, cracking behavior, and crystallographic texture of IN939 fabricated by powder bed fusion-laser beam (PBF-LB) method. Although both aged samples demonstrated similar grain structure and recrystallization behavior according to the electron backscatter diffraction (EBSD) analysis, as well as the precipitation of bimodal gamma ' phase and MC- and M23C6-type carbides, notable differences were observed in the size and morphology, particularly the gamma ' phase. The HT1 sample displayed coarsened primary gamma ' phase, with sizes reaching up to 2 mu m and exhibiting varied morphologies, including irregular and cuboidal shapes. Additionally, this treatment led to the formation of some gamma '-gamma eutectic regions and plate-like eta phase, along with the decomposition of MC-type carbides into M23C6-type carbides. In contrast, the HT2 sample displayed uniformly distributed spherical primary gamma ' phase with sizes ranging from 70 to 120 nm, accompanied by very fine secondary gamma ' phase. Furthermore, it was found that changes in both aged sample microstructures could result in the formation of strain-age cracks due to the gamma ' phase formation and liquation cracks due to the partial remelting of lower melting point phases. The findings also revealed that with the application of aging treatments, the hardness of the as-fabricated sample (339.8 +/- 3.4 HV) increased to 440.2 +/- 5.6 HV and 508.1 +/- 4.8 HV for the heat treatment of HT1 and HT2, respectively.Article Citation - WoS: 46Citation - Scopus: 49Recrystallization and Grain Growth Kinetics of In718 Manufactured by Laser Powder Bed Fusion(Elsevier, 2022) Dogu, Merve Nur; Davut, Kemal; Obeidi, Muhannad Ahmed; Yalcin, Mustafa Alp; Gu, Hengfeng; Low, Thaddeus Song En; Brabazon, DermotThe recrystallization and grain growth behaviour of IN718 alloy additively manufactured by laser powder bed fusion (L-PBF) is presented herein. The effects of three different temperatures (1050, 1150 and 1250 degrees C) and holding times (15, 45 and 90 min) were investigated. The texture evolution of the samples was recorded via electron backscatter diffraction (EBSD). The as-built sample is composed of bowl-shaped melt pools, a chessboard-like grain pattern and has a cube texture {100}<001>. Recrystallized grains were observed in the samples treated at 1150 degrees C for 15 min, as well as the samples treated for longer periods and at higher temperatures. Recrystallization was observed to start from high dislocation density regions, including the overlapping melt pools and the borders of the chessboard-like pattern. The initial cube texture transforms into a first-generation cube-twin texture {122}<212> via a twinning-assisted recrystallization mechanism. Then, those recrystallization nuclei sweep through the high defect density matrix; during which almost no new twins are formed. The samples treated at 1250 degrees C are almost completely recrystallized, which forms a weaker cube texture and a stronger P-orientation {011}<112>. However, the growth of recrystallized grains is very limited due to the presence of non-coherent precipitates. (C) 2022 The Author(s). Published by Elsevier B.V.Article Citation - WoS: 6Citation - Scopus: 8Topological Derivative Based Optimization of 3d Porous Elastic Microstructures(Elsevier Science Bv, 2014) Ozdemir, IzzetAs an alternative to the well established microstructural optimization techniques, topological derivative based optimization framework has been proposed and successfully implemented for tailoring/optimizing 2D elastic composites recently, Amstutz et al. [1]. In this paper, an optimization framework for 3D porous elastic microstructures is presented which is based on the notion of topological derivative and the computational homogenization of elastic composites. The sensitivity of the homogenized elasticity tensor to the insertion of infinitesimal hollow spheres within the elastic microstructure is used as the measure for the finite element based evolutionary optimization algorithm. The capabilities of the proposed framework, which is free of any regularization parameter, is assessed by means of example problems including some comparisons with analytical bounds. (C) 2013 Elsevier B.V. All rights reserved.Article Citation - WoS: 4Citation - Scopus: 6A Study on Microstructural Characterization of the Interface Between Apatite-Wollastonite Based Glass Ceramic and Feldspathic Dental Porcelain(Elsevier Sci Ltd, 2016) Pekkan, Gurel; Pekkan, Keriman; Park, Jongee; Ozturk, AbdullahIn this study, the contact area between the glass ceramic containing apatite [Ca-10(PO4)6(O,F-2)] and wollastonite [CaO center dot SiO2] crystals (A-W glass ceramic) and feldspathic dental porcelain was characterized using scanning electron microscope and energy dispersive spectroscopy. Alumina-added A W glass ceramics were prepared by sintering glass compacts in the MgO-CaO-SiO2-P2O5-Al2O3 system at 1100 degrees C. Commercially available dental porcelains for alumina frameworks were applied on the A-W glass ceramic specimen by brushing and carving, and then fired at 960 degrees C using an electrically heated vacuum-furnace. Results revealed that veneering of feldspathic dental porcelain on alumina-added A-W glass ceramic is possible by an interaction between them, with which a diffusion process involving i) seperation of the phases forming the alumina-added A-W glass ceramic, ii) chemical diffusion of elements between alumina-added A-W glass ceramic and feldspathic dental porcelain, and iii) formation of an interface layer, is taking place. The system studied has interfacial characteristics similar to the commercially available dental materials currently used in restorative dentistry. Hence, it may be further processed for potential clinical applications.Article Citation - WoS: 34Citation - Scopus: 34Friction Stir Processing of Dual Phase Steel: Microstructural Evolution and Mechanical Properties(Elsevier Science inc, 2019) Aktarer, S. M.; Kucukomeroglu, T.; Davut, K.The influence of friction stir processing (FSP) on the microstructure and mechanical properties of a DP 600 steel has been studied. The microstructure evolution during the FSP has been characterized using electron back scatter diffraction (EBSD) technique and scanning and transmission electron microscopes. Standard tension and hardness tests were used to characterize the mechanical properties. The results show that the FSP produced a refined microstructure composed of ferrite, bainite, martensite, and tempered martensite which in turn increased the hardness and strength magnitudes by a factor of 1.5. The initially 2.83 mu m average grain size of ferrite has decreased to 0.79 mu m in the pin effected zone of (PE-SZ-I) of the processed region. Both EBSD and TEM observations showed regions with high dislocation density and sub-structures region in the processed zone. The grain size became coarser, the density of both dislocations and low-angle grain boundaries decrease, away from the processed zone. Moreover, phase fractions and hardness values were predicted using CALPHAD thermodynamic based software based on commercial material properties. Although the prediction does not take into consideration the influence of severe plastic deformation, the results were within 10% uncertainties of the experimental findings. The present study demonstrates that an ultra-fine grained structure can be obtained through the thickness of a 1.5 mm thick D P600 steel sheet via FSP. FSP can produce a range of different hardness and strength values; which can also be predicted successfully by inputting the composition and local temperatures reached during the FSP.Article Citation - WoS: 123Citation - Scopus: 135Wire arc additive manufacturing of high-strength low alloy steels: study of process parameters and their influence on the bead geometry and mechanical characteristics(Springer London Ltd, 2020) Yildiz, Ahmet Suat; Davut, Kemal; Koc, Baris; Yilmaz, OguzhanAdditive manufacturing (AM) is becoming increasingly popular since it offers flexibility to produce complex designs with less tooling and minimum material at shorter lead times. Wire arc additive manufacturing (WAAM) is a variant of additive manufacturing which allows economical production of large-scale and high-density parts. The WAAM process has been studied extensively on different steels; however, the influence of process parameters, specifically wire feed speed (WFS), travel speed (TS), and their ratio on bead geometry, microstructure, and mechanical properties, are yet to be studied. The present work aims at closing this gap by using the WAAM process with robotic cold metal transfer (CMT) technology to manufacture high-strength structural steel parts. For that purpose, single-bead welds were produced from HSLA steel by varying WFS between 5 and 10 m/min and the WFS to TS ratio between 10 and 20. Those variations produce heat inputs in the range of 266-619 J/mm. The results have shown that the wire feed speed to travel speed ratio is the major parameter to control the heat input. Increasing heat input increases characteristic bead dimension, whereas it reduces the hardness. In the second part of experiments, two single-bead walls were deposited via the parallel deposition strategy and one multiple-bead wall was produced using the oscillation strategy. The tensile properties were tested along two directions: parallel and perpendicular to deposition directions. For the yield strength and tensile strength, the difference between horizontally and vertically tested specimens was smaller than the standard deviations. On the other hand, the total and uniform elongation values exhibit up to 10% difference in the test direction, indicating anisotropy in ductility. Those tensile properties were attributed to repeated thermal cycles during the WAMM process, which can cause heat transfer in multiple directions. The yield strength of the multiple-bead wall produced via oscillation was lower, whereas its ductility was higher. The tensile properties and hardness differences were found to correlate well with the microstructure.Article Microstructure-Based Prediction of Mechanical Properties of Austempered Ductile Iron Using Multiple Linear Regression Analysis(Springer Int Publ AG, 2025) Yalcin, M. Alp; Davut, KemalMultiple linear regression analysis (MLRA) was used to predict the mechanical properties of austempered ductile iron (ADI) including yield and tensile strength, uniform elongation, hardening exponent, as well as fracture energy by building a model that uses characteristic features of microstructural constituents as input parameters. The complex multi-scale microstructure of ADI, which is composed of spherical graphite particles over 10 mu m diameter; and an ausferritic matrix with sub-micron sized features, makes it ideal for prediction of mechanical properties. For that purpose, low alloyed ductile iron samples austempered between 300 and 400 degrees C for 45-180 min were tensile tested, and also multi-scale microstructural characterization were carried out using optical microscope, SEM, and EBSD technique. Moreover, a sensitivity analysis was performed to determine which microstructural parameter(s) each mechanical property is most sensitive to. The results show that tensile and yield strength are most sensitive to size and morphology of matrix phases. Moreover, the size and aspect ratio of acicular ferrite correlate well with those of high-carbon austenite; since both form during transformation of parent austenite into ausferrite during austempering treatment. Equiaxed parent austenite grains transform into ausferrite with acicular morphology during the austempering treatment; and presence of equiaxed austenite grains in the austempered samples indicates untransformed regions during austempering treatment. Ductility was found to be more sensitive to nodularity of graphite particles, and this sensitivity was attributed to the size difference between graphite particles and grain size of matrix phases.Article Citation - WoS: 24Citation - Scopus: 25Microstructural and Texture Evolution During Thermo-Hydrogen Processing of Ti6al4v Alloys Produced by Electron Beam Melting(Elsevier Science inc, 2020) Dogu, Merve Nur; Esen, Ziya; Davut, Kemal; Tan, Evren; Gumus, Berkay; Dericioglu, Arcan F.The present study was conducted to reveal the effects of building angles and post heat-treatments (2-step Thermo-Hydrogen Processing (THP) and conventional annealing treatment) on the density, microstructure and texture of Ti6Al4V alloy parts produced by Electron Beam Melting (EBM). The results showed that regardless of the building angle; the density, microstructure and crystallographic texture (defined with respect to building angle) of the as-produced samples were identical; having Widmanstatten a structure and columnar beta-grains which are parallel to building direction. The main texture component for the alpha phase was (10 (1) over bar0)//building direction, and for beta phase (001)//building or heat flow direction. The first step of THP, namely, the hydrogenation step, produced a needle-like microstructure and increased the local misorientations due to lattice distortion. On the other hand, after application of the second step of THP, dehydrogenation step, microstructure was refined, particularly alpha-grains that were larger than 10 mu m and located at grain boundaries. Moreover, THP randomized the crystallographic texture since it involves beta to alpha phase transformation, at which one beta-grain can produce 12 distinct alpha-variants. The grain boundary misorientation distributions also changed in accordance with the microstructural changes during the 2-step THP. On the other hand, annealing coarsened the grain boundary and Widmanstatten alpha phases; moreover, it changed the texture so that the basal planes (0001) rotated 30 degrees around the building direction.Article Citation - Scopus: 2Simulation Trends in Quenching Technology for Automotive Components(Maney Publishing, 2014) Felde,I.; Simsir,C.Quenching technology is widely used in automotive industry from a simple immersion quenching of gears up to the complex production technology of press hardening. The selection of process parameters to develop the desired properties is challenging due to the complexity of the physical phenomena occurring during the manufacturing cycle. In the last decades several computational methods have been applied successful to optimise the heat treatment processes. This paper is focusing on some examples demonstrating the state of the art of the simulation tools, including the physical phenomena of quenching, the theoretical background of the coupled models used for estimation the microstructure, mechanical properties and deformation of heat treated automotive components. © 2014 IHTSE Partnership.Article Citation - WoS: 11Citation - Scopus: 17Machinability Evaluations of Austempered Ductile Iron and Cast Steel With Similar Mechanical Properties Under Eco-Friendly Milling Conditions(Elsevier, 2021) Eraslan, Dogancan; Balci, Ahmet; Cetin, Baris; Ucak, Necati; Cicek, Adem; Yilmaz, Okan Deniz; Davut, KemalIn engineering applications, to increase productivity and to decrease production costs, the selection of the proper engineering material is essential. At that point, machining operations directly affect the production costs. Therefore, determination of the material with the desired mechanical properties and easy-to-cut characteristics has a critical importance. This situation is currently gaining more importance in especially defense industry applications in which high strength engineering materials are heavily employed. In addition, tool performance and final product quality are directly influenced by the cooling and/or lubrication conditions in particularly interrupted cutting operations. In this study, machinability characteristics of G18NiMoCr3-6+QT1 cast steel (CS) and 1050-6 austempered ductile iron (ADI) with similar mechanical properties during milling operations were investigated. The tests were performed using TiAlN coated cemented carbide (WC-Co) end mills under dry, conventional cutting fluid (CCF), and minimum quantity lubrication (MQL) conditions. Under each condition, the variations of cutting forces, tool wear, average surface roughness (Ra), and subsurface microstructure and microhardness were analyzed for both materials and then compared to one another. Test results showed that 1050-6 ADI led to further tool wear in comparison to G18NiMoCr3-6+QT1 CS. According to obtained results, dry condition is more favorable than CCF and MQL conditions in terms of cutting forces, surface roughness, and tool wear for both types of material. In addition, examinations on subsurface microstructures showed that MQL conditions provided an effective cutting environment to maintain microstructural stability of workpiece materials. (c) 2021 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
