Doğu, Merve Nur

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Citation - WoS: 24
Citation - Scopus: 27
Effect of Solution Heat Treatment on the Microstructure and Crystallographic Texture of In939 Fabricated by Powder Bed Fusion-Laser Beam
(Elsevier, 2023) Dogu, Merve Nur; Ozer, Seren; Yalcin, Mustafa Alp; Davut, Kemal; Bilgin, Guney Mert; Obeidi, Muhannad Ahmed; Brabazon, Dermot
The effect of various solution heat treatment temperatures (i.e., 1120, 1160, 1200 and 1240 & DEG;C) on the microstructure, grain morphology and crystallographic texture of IN939 fabricated by powder bed fusion-laser beam (PBF-LB) was investigated. Microstructural analyses showed that the high-temperature gradient and rapid solidification of the PBF-LB processing caused different resulting microstructures compared to conventionally pro-duced counterparts. The melt pool morphologies and laser scanning paths were examined in the as-fabricated samples in the XZ-and XY-planes, respectively. After the application of solution heat treatment at 1120 & DEG;C, the as-fabricated PBF-LB initial microstructure was still apparent. For solution heat treatments of 1200 & DEG;C and above, the melt pool and scanning path morphologies disappeared and converted into a mixture of columnar grains in the XZ-plane and equiaxed grains in the XY-plane. On the other hand, large equiaxed grains were observed when the samples were solutionized at 1240 & DEG;C. Additionally, g' phase precipitated within the matrix after all solution heat treatment conditions, which led to increase in the microhardness values. According to electron backscatter diffraction (EBSD) analyses, both as-fabricated and solution heat-treated samples had intense texture with {001} plane normal parallel to the building direction. The first recrystallized grains began to appear when the samples were subjected to the solution heat treatment at 1160 & DEG;C and the fraction of the recrystallized grains increased with increasing temperature, as supported by kernel average misorientation (KAM) and grain spread orientation (GOS) analyses.& COPY; 2023 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
Citation - WoS: 13
Citation - Scopus: 13
A Comprehensive Characterization of the Effect of Spatter Powder on In939 Parts Fabricated by Laser Powder Bed Fusion
(Elsevier Sci Ltd, 2023) Dogu, Merve Nur; Mussatto, Andre; Yalcin, Mustafa Alp; Ozer, Seren; Davut, Kemal; Obeidi, Muhannad Ahmed; Brabazon, Dermot
This study is focused on a comprehensive characterization of virgin and spatter IN939 powders and the effects of a certain amount of spatter powder on the part quality of IN939 fabricated by the L-PBF process. A brown tint coloration formed Al2O3 oxide, pores, a 124.4% increase in the average particle size, a 10.2% decrease in the powder circularity, and a 7.5% decrease in the powder aspect ratio were observed in the spatter powder. Additionally, higher average grain size and lower nanohardness were obtained for the spatter powder. In order to understand the effect of a certain amount of spatter powder on the part quality, 10 wt% spatter powder was mixed with the virgin powder. This addition was found to decrease the flowability of the powder. Moreover, this addition decreased relative density by around 0.3% and increased surface roughness by around 80.8% in the fabricated samples (termed as V and SV). On the other hand, there was no considerable microstructural, texture, microhardness, and nanohardness difference between V and SV samples, although the spatter powder addition caused a 30.2% increase in the average grain size of SV. The overall texture for both V and SV samples exhibit (00 1)//BD.

Journal	Count
Journal of Materials Research and Technology	3
Materials & Design	1
Materials Characterization	1
Materials Today Communications	1
SSRN Electronic Journal	1

Doğu, Merve Nur

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